Synthesis, characterization and crystal structures of [Mo(CO)4]2TPTA and [W(CO)4]2TPTA (TPTA = 1,4,8,11-tetrakis(methyldiphenylphosphino)-1,4,8,11-tetraazacyclotetradecane)
Identifieur interne : 002F27 ( Main/Exploration ); précédent : 002F26; suivant : 002F28Synthesis, characterization and crystal structures of [Mo(CO)4]2TPTA and [W(CO)4]2TPTA (TPTA = 1,4,8,11-tetrakis(methyldiphenylphosphino)-1,4,8,11-tetraazacyclotetradecane)
Auteurs : Dubravka Matkovi Alogovi [Croatie] ; Henrika Meider [Croatie] ; Pavica Planini [Croatie]Source :
- Journal of Organometallic Chemistry [ 0022-328X ] ; 1993.
Abstract
1,4,8,11-Tetrakis(methyldiphenylphosphino)-1,4,8,11-tetraazacyclotetradecane (TPTA) reacts with molybdenum(0) and tungsten(0) hexacarbonyls to give yellow crystalline diamagnetic complexes of the formula [M(CO)4]2TPTA. Each metal atom in these binuclear species is coordinated by two phosphorus atoms from the pendant methyldiphenylphosphino groups and by four carbonyls in a cis octahedral arrangement.
Url:
DOI: 10.1016/0022-328X(93)83283-2
Affiliations:
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